Triethylamine → HCID 20322094, 화합물

HRID 839814노트

반응식

HRID 839814 반응식
[CH2:1]([O:3][CH:4]([O:7][CH2:8][CH3:9])[CH2:5][NH2:6])[CH3:2].Br[CH2:11][CH:12]1[O:17][CH2:16][CH2:15][CH2:14][O:13]1.C(N(CC)CC)C>C1(C)C=CC=CC=1>[CH2:1]([O:3][CH:4]([O:7][CH2:8][CH3:9])[CH2:5][NH:6][CH2:11][CH:12]1[O:17][CH2:16][CH2:15][CH2:14][O:13]1)[CH3:2]

참가 물질

5

반응물 3

HCID 8471TriethylamineHCID 695242,2-DiethoxyethylamineHCID 3036832-Bromomethyl-1,3-dioxane

생성물 1

HCID 20322094HCID 20322094, 화합물

시약·촉매·용매 1

HCID 1140Toluene용매

실험 절차

2,2-Diethoxyethylamine (23.3 grams), 2-bromomethyl-1,3-dioxane (29.2 grams), triethylamine (25 ml) and toluene (150 ml) are charged into a glass reaction vessel equipped with a mechanical stirrer, thermometer and reflux condenser. The reaction mixture is heated at reflux overnight. After this time the mixture is cooled and filtered. The filtrate is then distilled under reduced pressure to yield the desired product N-(2,2-diethoxyethyl)-N-(1,3-dioxan-2-ylmethyl)amine.

후처리

  1. customequipped with a mechanical stirrer
  2. temperaturethermometer and reflux condenser
  3. temperatureThe reaction mixture is heated
  4. temperatureat reflux overnight
  5. temperatureAfter this time the mixture is cooled
  6. filtrationfiltered
  7. distillationThe filtrate is then distilled under reduced pressure

출처 및 근거

ORD 기록
ord-ce262f535bd5422b949724e8ffee2c25
출처 데이터셋
uspto-grants-1978_06
특허 번호
US04097491

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