Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzyl Bromide → 3-Phenyl-5-(3-phenylpropyl)isoxazole-4-carboxylic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzyl Bromide | HCID 7498 | — |
| 반응물 | 3-Phenyl-5-(2-phenylethyl)isoxazole-4-carboxylic acid | HCID 23447906 | — |
| 생성물 | 3-Phenyl-5-(3-phenylpropyl)isoxazole-4-carboxylic acid | HCID 23447887 | 72% |
반응 단계
The title compound was prepared as described for Compound 28A but substituting 2-phenylethylbromide for benzyl bromide. The crude was purified by flash chromatography (ethyl acetate-petroleum ether-acetic acid 1:1:0.01 mL) to afford the title compound (72%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06365591B1 |
| 출처 데이터셋 | uspto-grants-2002_04 |
| ORD ID | ord-5384ec8b06e24c5a8f96afdfd5615e71 |
| 출처 메모 | uspto-grants-2002_04 |