Sulfacetamide → HCID 178475155, 화합물

HRID 840881

반응식

HRID 840881 반응식
C(O[CH:4]=[C:5]1[C:16]2[C:8](=[CH:9][CH:10]=[C:11]3[C:15]=2[S:14][CH:13]=[N:12]3)[NH:7][C:6]1=[O:17])C.[C:18]([NH:21][S:22]([C:25]1[CH:30]=[CH:29][C:28]([NH2:31])=[CH:27][CH:26]=1)(=[O:24])=[O:23])(=[O:20])[CH3:19]>>[C:18]([NH:21][S:22]([C:25]1[CH:30]=[CH:29][C:28]([NH:31][CH:4]=[C:5]2[C:16]3[C:8](=[CH:9][CH:10]=[C:11]4[C:15]=3[S:14][CH:13]=[N:12]4)[NH:7][C:6]2=[O:17])=[CH:27][CH:26]=1)(=[O:24])=[O:23])(=[O:20])[CH3:19]

참가 물질

3

반응물 2

HCID 5320SulfacetamideHCID 539908078-[Ethoxymethylidene]-6H-[1,3]thiazolo[5,4-e]indol-7-one

생성물 1

HCID 178475155HCID 178475155, 화합물수율 26%

실험 절차

The title compound was prepared in 26% yield from 8-ethoxymethylene-6,8-dihydro-1-thia-3,6-diaza-as-indacen-7-one and N-acetyl-4-aminobenzenesulfonamide according to Procedure J: 1H NMR (DMSO-d6): δ12.0 (s, 1H), 11.2 (d, 1H), 10.9 (s, 1H), 8.1 (d, 1H), 7.9 (m, 3H), 7.6 (d, 2H), 7.1 (d, 1H), 2.0 (s, 3H); ESI−MS m/z413 (M−H)−.

출처 및 근거

ORD 기록
ord-c6e9c057838f45d080e8f856c66b1673
출처 데이터셋
uspto-grants-2002_04
특허 번호
US06369086B1

연결된 노트

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