Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzylamine → HCID 178418897, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzylamine | HCID 7504 | — |
| 반응물 | Ethyl thiocyanate | HCID 10968 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Trimethylsilyl triflate | HCID 65367 | — |
| 생성물 | HCID 178418897 | HCID 178418897 | 100% |
반응 단계
Benzylamine (13.8 mg) was dissolved in ethyl thiocyanate (50 μl). To this solution, trimethylsilyl trifluoromethanesulfonate (25.7 μl) was added dropwise at room temperature. After continued stirring for 1 day at room temperature, 2N aqueous sodium hydroxide was added to the solution, which was then extracted with ethyl acetate. The ethyl acetate layer was dried over anhydrous sodium sulfate and concentrated under reduced pressure to give the titled compound (25.4 mg, yield 100%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07087783B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-7db99835b713471dac9c78ee60d5003c |
| 출처 메모 | uspto-grants-2006_08 |