Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanol → Canthaxanthin
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | Water | HCID 962 | — |
| 반응물 | Chloroform | HCID 6212 | — |
| 반응물 | Beta-Carotene | HCID 5280489 | — |
| 생성물 | Canthaxanthin | HCID 5281227 | 85% |
반응 단계
Into a flask was charged 0.5 gm of β-carotene and 10 ml of chloroform. The mixture is stirred to form a solution. Into this solution was charged 1.6 ml of the oxidant solution described in example 1. The mixture was stirred for 1.5 hours to complete the reaction. The phases were separated and the organic phase was washed with water once and evaporated to yield a residue that was dissolved in 10 ml of warm ethanol. This ethanol solution was added slowly to 50 ml of water to form a precipitate which was filtered and dried to yield 85% yield of canthaxanthin of approximately 80% purity.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06372946B1 |
| 출처 데이터셋 | uspto-grants-2002_04 |
| ORD ID | ord-bbaa20909ddd4b8a880e98272433b08a |
| 출처 메모 | uspto-grants-2002_04 |