HCID 178478098, 화합물 → HCID 178420213, 화합물
반응식
Cl[C:2]1[CH:7]=[CH:6][CH:5]=[C:4](Cl)[C:3]=1[CH2:9][C:10]1[NH:14][N:13]=[N:12][N:11]=1>[Pd].CO>[C:3]1([CH2:9][C:10]2[NH:14][N:13]=[N:12][N:11]=2)[CH:2]=[CH:7][CH:6]=[CH:5][CH:4]=1참가 물질
4
실험 절차
The mixture of 5-(2,6-dichlorophenylmethyl)tetrazole (355 mg), 5% palladium on activated carbon (93 mg) and methanol (8 ml) was stirred for 1 h room temperature under an atmosphere of hydrogen gas. The reaction mixture was filtered through Celite (trade mark) and the filtrate was concentrated to give the title compound having the following physical data.
후처리
- filtrationThe reaction mixture was filtered through Celite (trade mark)
- concentrationthe filtrate was concentrated
출처 및 근거
- ORD 기록
- ord-dbca2720337a4c9a98eaadeb62c55c46
- 출처 데이터셋
- uspto-grants-2002_04
- 특허 번호
- US06376484B1
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