Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → Astaxanthin
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | Sodium Iodide | HCID 5238 | — |
| 반응물 | Sodium Chlorate | HCID 516902 | — |
| 반응물 | Zeaxanthin | HCID 5280899 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | Astaxanthin | HCID 5281224 | — |
반응 단계
Zeaxanthin (50 mg) was stirred in 20 ml of chloroform under nitrogen. To this stirred mixture, 200 mg of sodium chlorate and 50 mg of sodium iodide in 10 ml of water was added. The mixture was acidified slowly with 1 ml of 27% sulfuric acid. The reaction was stirred at room temperature. After 5 hours, a significant quantity of astaxanthin had formed. The reaction was worked up by addition of 1 ml of 40% sodium hydroxide, separation of the organic solution and evaporation to yield astaxanthin.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06376717B2 |
| 출처 데이터셋 | uspto-grants-2002_04 |
| ORD ID | ord-5a002155ec6d4801ac300abd4f20e80b |
| 출처 메모 | uspto-grants-2002_04 |