Methanesulfonyl chloride → 1-(Chloromethyl)-3-fluoro-2-methoxybenzene
반응식
S([Cl:5])(C)(=O)=O.[F:6][C:7]1[C:8]([O:15][CH3:16])=[C:9]([CH2:13]O)[CH:10]=[CH:11][CH:12]=1>>[Cl:5][CH2:13][C:9]1[CH:10]=[CH:11][CH:12]=[C:7]([F:6])[C:8]=1[O:15][CH3:16]참가 물질
3
실험 절차
In an analogous manner to that described in (γ) (3-fluoro-2-methoxy-phenyl)-methanol was treated with mesylchloride to obtain 1-chloromethyl-3-fluoro-2-methoxy-benzene as a colorless liquid; MS: 174 (M)+.
출처 및 근거
- ORD 기록
- ord-ea93d8410ced4a278d55f4af08f92629
- 출처 데이터셋
- uspto-grants-2002_04
- 특허 번호
- US06376672B1
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