Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → 4-Cyclohexylbutanoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | Cyclohexanebutanoic acid | HCID 75200 | — |
| 생성물 | 4-Cyclohexylbutanoyl chloride | HCID 13315625 | — |
반응 단계
50 g of 4-cyclohexanebutyric acid are refluxed for 4 hours in 160 ml of thionyl chloride. After evaporation of the excess thionyl chloride, the expected product is distilled off. b.p.=70-80° C. at 400 Pa.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06380230B1 |
| 출처 데이터셋 | uspto-grants-2002_04 |
| ORD ID | ord-b67d361baaf844d68daab285fd9d6e54 |
| 출처 메모 | uspto-grants-2002_04 |