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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 84481생성일: 2026년 10월 25일

3-Pyridinemethanamine → N2-(2-chlorophenyl)-N2-methyl-N8-(pyridin-3-ylmethyl)-4,5-dihydrobenzo[b]thieno[2,3-d]oxepine-2,8-dicarboxamide

https://huagongshe.com/reaction/84481

반응식

참여 물질

역할이름HCID투입량
반응물3-PyridinemethanamineHCID 31018—
반응물2-[(2-Chloro-phenyl)-methyl-carbamoyl]-4,5-dihydro-6-oxa-1-thia-benzo[e]azulene-8-carboxylic acid methyl esterHCID 44242363—
생성물N2-(2-chlorophenyl)-N2-methyl-N8-(pyridin-3-ylmethyl)-4,5-dihydrobenzo[b]thieno[2,3-d]oxepine-2,8-dicarboxamideHCID 44242634—

반응 단계

Following Example 47 and General Procedure C, methyl 2-((2-chlorophenyl)(methyl)carbamoyl)-4,5-dihydrobenzo[b]thieno[2,3-d]oxepine-8-carboxylate 138 and 3-aminomethylpyridine gave 173. MS: (ESI+) 504.0

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US08846762B2
출처 데이터셋uspto-grants-2014_09
ORD IDord-93fe17cc42b8426fa6d31fbeb1fcc5b2
출처 메모uspto-grants-2014_09