Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Saccharin → Glycidyl methacrylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Saccharin | HCID 5143 | — |
| 반응물 | Dimethyl-p-toluidine | HCID 7471 | — |
| 반응물 | Dicyandiamide | HCID 10005 | — |
| 반응물 | Chlortoluron | HCID 27375 | — |
| 반응물 | Tert-butyl cumene peroxide | HCID 76997 | — |
| 반응물 | Phosphorohydrazidic acid, diethyl ester | HCID 143340 | — |
| 생성물 | Glycidyl methacrylate | HCID 7837 | — |
반응 단계
Mixure A (20.0 g) is mixed with dicyandiamide (0.4 g) and N-(3-chloro-4-methylphenyl)-N',N'-dimethylurea (0.4 g) and the mixture milled in a triple-roll mill until homogeneous. The milled product is then treated with tert.butyl cumyl peroxide (0.5 g), N,N-dimethyl-p-toluidine (0.1 g), o-benzoic sulphimide (0.1 g) and diethyl phosphoro hydrazidate (0.2 g) and mixed until homogeneous.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04755571 |
| 출처 데이터셋 | uspto-grants-1988_07 |
| ORD ID | ord-0e683cd1b9c24f10a8ff55d7aabcd417 |
| 출처 메모 | uspto-grants-1988_07 |