Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzaldehyde → 1-Cyclohexyl-4-dimethylamino-2-phenyl-2-buten-1-ol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzaldehyde | HCID 240 | — |
| 반응물 | beta-Diethylaminopropiophenone 2,4,6-triisopropylbenzenesulphonylhydrazone | HCID 86741730 | — |
| 생성물 | 1-Cyclohexyl-4-dimethylamino-2-phenyl-2-buten-1-ol | HCID 53845847 | — |
반응 단계
By using a method similar to that described in Example 22, but starting from β-diethylaminopropiophenone 2,4,6-triisopropylbenzenesulphonylhydrazone (30 g) and benzaldehyde (6.9 cc), 4-diethylamino-1,2-diphenyl-2-buten-1-ol (Z) hydrochloride (3.2 g) is obtained, after recrystallisation from acetone, in the form of white crystals melting at 140° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04755599 |
| 출처 데이터셋 | uspto-grants-1988_07 |
| ORD ID | ord-7e88a7e6b815446cb4810f2debc5f5bc |
| 출처 메모 | uspto-grants-1988_07 |