Ethyl 3-hydroxy-2-nitrobutanoate → HCID 54371401, 화합물

HRID 845242노트

반응식

HRID 845242 반응식
[CH2:1]([O:3][C:4]([C:6]1[N:7]=[CH:8][C:9]2[NH:10][C:11]3[C:16]([C:17]=2[C:18]=1[CH3:19])=[C:15]([CH2:20][OH:21])[CH:14]=[CH:13][CH:12]=3)=[O:5])[CH3:2].C(OC(=O)C([N+]([O-])=O)C(O)C)C>>[CH2:1]([O:3][C:4]([C:6]1[N:7]=[CH:8][C:9]2[NH:10][C:11]3[C:16]([C:17]=2[C:18]=1[CH3:19])=[C:15]([CH:20]=[O:21])[CH:14]=[CH:13][CH:12]=3)=[O:5])[CH3:2]

참가 물질

3

반응물 2

HCID 20470476Ethyl 3-hydroxy-2-nitrobutanoateHCID 53753831HCID 53753831, 화합물

생성물 1

HCID 54371401HCID 54371401, 화합물

실험 절차

The synthesis takes place according to the method described in example 1 from 5-hydroxymethyl-4-methyl-beta-carboline-3-carboxylic acid ethyl ester, which in turn is prepared according to example 2 from 2-nitro-3-hydroxybutyric acid ethyl ester in 5 stages.

후처리

  1. customis prepared

출처 및 근거

ORD 기록
ord-0c6dedb474a14471bb70bde7e54ffb97
출처 데이터셋
uspto-grants-1988_07
특허 번호
US04757070

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