Nitroethane → HCID 54489179, 화합물

HRID 845244노트

반응식

HRID 845244 반응식
C(OC(C1N=CC2NC3C(C=2C=1C)=C(C=O)C=CC=3)=O)C.[N+](CC)([O-])=O.[CH2:27]([O:29][C:30]([C:32]1[N:33]=[CH:34][C:35]2[NH:36][C:37]3[C:42]([C:43]=2[C:44]=1[CH3:45])=[C:41]([CH:46]=[C:47]([N+:49]([O-])=O)[CH3:48])[CH:40]=[CH:39][CH:38]=3)=[O:31])[CH3:28]>>[CH2:27]([O:29][C:30]([C:32]1[N:33]=[CH:34][C:35]2[NH:36][C:37]3[C:42]([C:43]=2[C:44]=1[CH3:45])=[C:41]([CH2:46][CH:47]([NH2:49])[CH3:48])[CH:40]=[CH:39][CH:38]=3)=[O:31])[CH3:28]

참가 물질

4

반응물 3

HCID 6587NitroethaneHCID 54371401HCID 54371401, 화합물HCID 54456541HCID 54456541, 화합물

생성물 1

HCID 54489179HCID 54489179, 화합물

실험 절차

The production takes places analogously to example 9 by condensation of 5-formyl-4-methyl-beta-carboline-3-carboxylic acid ethyl ester with nitroethane and hydrogenation of the resulting 4-methyl-5-(2-nitropropenyl)beta-carboline-3-carboxylic acid ethyl ester.

출처 및 근거

ORD 기록
ord-259f5003ceec4c7ba900d92ec2acb76b
출처 데이터셋
uspto-grants-1988_07
특허 번호
US04757070

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