반응식
[CH2:1]([N:8]([CH2:10][C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)[OH:9])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.CC(C)([O-])C.[K+].[C:23]([NH:31][C:32](=[O:35])[CH:33]=[CH2:34])([CH2:26][C:27]([CH3:30])([CH3:29])[CH3:28])([CH3:25])[CH3:24]>O1CCCC1>[C:23]([NH:31][C:32](=[O:35])[CH2:33][CH2:34][O:9][N:8]([CH2:1][C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1)[CH2:10][C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)([CH2:26][C:27]([CH3:28])([CH3:29])[CH3:30])([CH3:24])[CH3:25]참가 물질
5
실험 절차
The procedure of Example I is repeated using 23.31 g of dibenzylhydroxylamine, 1.23 g of potassium-tert-butoxide and 20.0 g of N-tert-octylacrylamide in 100 ml of dry tetrahydrofuran to afford the title compound as a white crystalline solid: mp 96°-98° C.
출처 및 근거
- ORD 기록
- ord-0a1301150065428bb24f377777dcbf8f
- 출처 데이터셋
- uspto-grants-1988_07
- 특허 번호
- US04760179
연결된 노트
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