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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 84600생성일: 2026년 10월 26일

Methyl iodide → Tert-butyl tert-butyl(2-((2-chlorophenyl)(methyl)carbamoyl)-4,5-dihydropyrido[4,3-b]thieno[2,3-d]oxepin-8-yl)carbamate

https://huagongshe.com/reaction/84600

반응식

참여 물질

역할이름HCID투입량
반응물Methyl iodideHCID 6328—
반응물Sodium hydrideHCID 24758—
반응물tert-Butyl tert-butyl(2-(2-chlorophenylcarbamoyl)-4,5-dihydropyrido[4,3-b]thieno[2,3-d]oxepin-8-yl)carbamateHCID 57900446—
생성물Tert-butyl tert-butyl(2-((2-chlorophenyl)(methyl)carbamoyl)-4,5-dihydropyrido[4,3-b]thieno[2,3-d]oxepin-8-yl)carbamateHCID 5790024978%

반응 단계

Following Scheme 4, tert-butyl tert-butyl(2-(2-chlorophenylcarbamoyl)-4,5-dihydropyrido[4,3-b]thieno[2,3-d]oxepin-8-yl)carbamate, methyl iodide and sodium hydride were reacted to give tert-butyl tert-butyl(2-((2-chlorophenyl)(methyl)carbamoyl)-4,5-dihydropyrido[4,3-b]thieno[2,3-d]oxepin-8-yl)carbamate (78%). MS: (ESI+) 542.3

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US08846762B2
출처 데이터셋uspto-grants-2014_09
ORD IDord-ff37a9b2120f4d91b597578651acbfb1
출처 메모uspto-grants-2014_09