Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Iodide → HCID 14856141, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Iodide | HCID 5238 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 1-(3-Chlorophenyl)piperazine monohydrochloride | HCID 25681 | — |
| 반응물 | 3-(4-Bromobutyl)-2-methyl-4-thiazolidinone | HCID 10490993 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | HCID 14856141 | HCID 14856141 | — |
반응 단계
To a solution of 2-methyl-3-(4-bromobutyl)-4-thiazolidinone (4.0 g) and 1-(3-chlorophenyl)piperazine hydrochloride (3.69 g) in 100 ml of dry CH3CN were added K2CO3 (8.8 g) and NaI (200 mg). The mixture was heated to reflux with stirring under N2.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05136037 |
| 출처 데이터셋 | uspto-grants-1992_08 |
| ORD ID | ord-84fe4d6908ce46b8876bfac3ff95b15b |
| 출처 메모 | uspto-grants-1992_08 |