Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3,3-Dimethoxy-pyrrolidine benzyl carbamate → 3,3-Dimethoxypyrrolidine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3,3-Dimethoxy-pyrrolidine benzyl carbamate | HCID 86746061 | — |
| 반응물 | HCID 178418361 | HCID 178418361 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 3,3-Dimethoxypyrrolidine | HCID 11029882 | — |
반응 단계
The 2.21 g of 3,3-dimethoxy-pyrrolidine benzyl carbamate, from step 3, dissolved in 100 mL of methanol, 2.21 g of Pd/C (wet) was added, and placed under 4 atm of hydrogen for 20 hours. The catalyst was filtered off using a 0.45 micro millipore filter and the solvent was evaporated to afford the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05137892 |
| 출처 데이터셋 | uspto-grants-1992_08 |
| ORD ID | ord-8db8cb3449b64d54a778053f320dfcbb |
| 출처 메모 | uspto-grants-1992_08 |