Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Isobutyramide → [1-Dimethylamino-meth-(e)-ylidene]-isobutyramide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Isobutyramide | HCID 68424 | — |
| 반응물 | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| 생성물 | [1-Dimethylamino-meth-(e)-ylidene]-isobutyramide | HCID 87184356 | — |
반응 단계
Following the procedure for 449, Step 3, isobutyramide was reacted with DMF-DMA to afford the title compound as a yellow oil. 1H NMR (CDCl3): 8.39 (1 H, s), 3.10 (3 H, m), 3.07 (3 H, d, J=0.67 Hz), 2.68-2.56 (1 H, m), 1.17 (3 H, s), 1.18-1.11 (3 H, s).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08846762B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-07cbee89ad884b72a7c66f70640ceb4a |
| 출처 메모 | uspto-grants-2014_09 |