Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Dodecanethiol → Ethyl Acrylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Dodecanethiol | HCID 8195 | — |
| 반응물 | Tert-butyl 2-ethyl-2-methylheptaneperoxoate | HCID 71359725 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | Ethyl Acrylate | HCID 8821 | — |
| 생성물 | Decyl methacrylate | HCID 18510 | — |
반응 단계
350 g of toluene, 135 g of ethyl acrylate, and 15 g of n-decyl methacrylate were polymerized with stirring in a reaction flask at 50°-60° C. under argon with 0.3 g of dodecyl mercaptan as a regulator and 2 g of t-butyl perneodecanoate as initiator. After about 30 minutes of reaction, the mixture was precipitated in methanol and the polymer was dried under vacuum.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05141993 |
| 출처 데이터셋 | uspto-grants-1992_08 |
| ORD ID | ord-c2b49c75adc9482d84cd3eef32fdd950 |
| 출처 메모 | uspto-grants-1992_08 |