Formaldehyde → HCID 22910140, 화합물

HRID 847625노트

반응식

HRID 847625 반응식
[OH:1][CH:2]([CH:11]([OH:20])[CH2:12][CH2:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)[CH2:3][CH2:4][C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1.[CH2:21]=O.OS(O)(=O)=O>C(O)(=O)C>[C:5]1([CH2:4][CH2:3][CH:2]2[CH:11]([CH2:12][CH2:13][C:14]3[CH:15]=[CH:16][CH:17]=[CH:18][CH:19]=3)[O:20][CH2:21][O:1]2)[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1

참가 물질

5

반응물 3

HCID 712FormaldehydeHCID 1118Sulfuric AcidHCID 114145663,4-Hexanediol, 1,6-diphenyl-

생성물 1

HCID 22910140HCID 22910140, 화합물

시약·촉매·용매 1

HCID 176Acetic Acid용매

실험 절차

The resultant compound of Example 149 was treated with paraformaldehyde and H2SO4 in acetic acid according to the procedure of Hough, et. al. (J. Chem. Soc., 1952, 1525) to provide the desired compound.

출처 및 근거

ORD 기록
ord-304dbfa286484d54aae0f26bcf80e877
출처 데이터셋
uspto-grants-1992_08
특허 번호
US05142056

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