Sulfuric Acid → 4-Amino-3-nitrobenzophenone

HRID 847752

반응식

HRID 847752 반응식
C([NH:4][C:5]1[CH:18]=[CH:17][C:8]([C:9]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)=[O:10])=[CH:7][C:6]=1[N+:19]([O-:21])=[O:20])(=O)C.S(=O)(=O)(O)O>>[NH2:4][C:5]1[CH:18]=[CH:17][C:8]([C:9]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)=[O:10])=[CH:7][C:6]=1[N+:19]([O-:21])=[O:20]

참가 물질

3

반응물 2

HCID 1118Sulfuric AcidHCID 5969694-Acetamido-3-nitrobenzophenone

생성물 1

HCID 5969704-Amino-3-nitrobenzophenone

실험 절차

Ten grams of 4-acetamido-3-nitrobenzophenone was added protion-wise to 40 ml. of sulfuric acid. The reaction temperature was moderated with a water bath. After stirring about 45 minutes the reaction mixture was carefully poured over ice. The precipitated product was filtered to yield 4-amino-3-nitrobenzophenone.

후처리

  1. customThe reaction temperature was moderated with a water bath
  2. additionwas carefully poured over ice
  3. filtrationThe precipitated product was filtered

출처 및 근거

ORD 기록
ord-bc707c7fad8441428688b045f3e0ff4b
출처 데이터셋
uspto-grants-1981_10
특허 번호
US04293558

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