N,N-Diethylethylenediamine → HCID 20565488, 화합물

반응식

Cl[C:2]1[C:7](=[O:8])[N:6]([C:9]2[CH:14]=[CH:13][C:12]([O:15][CH3:16])=[CH:11][CH:10]=2)[C:5]2[N:17]=[CH:18][CH:19]=[CH:20][C:4]=2[N:3]=1.[CH2:21]([N:23]([CH2:27][CH3:28])[CH2:24][CH2:25][NH2:26])[CH3:22]>>[CH2:21]([N:23]([CH2:24][CH2:25][NH:26][C:2]1[C:7](=[O:8])[N:6]([C:9]2[CH:14]=[CH:13][C:12]([O:15][CH3:16])=[CH:11][CH:10]=2)[C:5]2[N:17]=[CH:18][CH:19]=[CH:20][C:4]=2[N:3]=1)[CH2:27][CH3:28])[CH3:22]

참가 물질

반응물 2

HCID 60993N,N-Diethylethylenediamine

HCID 20565438HCID 20565438, 화합물

생성물 1

HCID 20565488HCID 20565488, 화합물

실험 절차

Preparation as in Example 39 but using 2-chloro-3,4-dihydro-4-(4-methoxyphenyl)-3-oxopyrido[2,3-b]pyrazine and N,N-diethylethylene diamine gave the title compound mp 167°-168° C.

후처리

customPreparation as in Example 39

출처 및 근거

ORD 기록: ord-c7b9f8948b9a4613a39c9acc6da49649
출처 데이터셋: uspto-grants-1981_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04296114

반응 노트

불러오는 중…