Ethylene → n-Dodecylethyldichlorosilane

HRID 848822

반응식

HRID 848822 반응식
[CH2:1]([SiH:13]([Cl:15])[Cl:14])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[CH2:16]=[CH2:17]>C(O)(C)C>[CH2:1]([Si:13]([CH2:16][CH3:17])([Cl:15])[Cl:14])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

참가 물질

4

반응물 2

HCID 6325EthyleneHCID 123720552n-Dodecyldichlorosilane

생성물 1

HCID 20564956n-Dodecylethyldichlorosilane

시약·촉매·용매 1

HCID 3776Isopropanol용매

실험 절차

Resultant n-dodecyldichlorosilane in an amount of 161.4 g (0.6 mol), 22.4 g of ethylene (0.8 mol) and a solution of H2PtCl6 ·6H2O in isopropanol (0.05 mol % relative to n-dodecyldichlorosilane) were charged in a pressure-proof stainless steel reactor. After sealing, reaction was carried out at 50° C. for 25 hours to give n-dodecylethyldichlorosilane [(n--C12H25)(C2H5)SiCl2 ].

후처리

  1. customreaction

출처 및 근거

ORD 기록
ord-3fda26a631f947ffb97d341e6f053fd4
출처 데이터셋
uspto-grants-1981_10
특허 번호
US04297499

연결된 노트

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