Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Octadecene → Octadecyldichlorosilane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Octadecene | HCID 8217 | — |
| 반응물 | Dichlorosilane | HCID 61330 | — |
| 생성물 | Octadecyldichlorosilane | HCID 102243275 | — |
반응 단계
Dichlorosilane in an amount of 60.6 g (0.6 mol), 176.4 g of 1-octadecene (0.7 mol) and 0.07 mol % of RhCl(PPh)3 (relative to dichlorosilane) were charged in a 500 ml pressure-proof stainless steel reactor. After sealing, reaction was carried out at 130° C. for 30 hours. The reacted liquid was distilled in vacuo to give n-octadecyldichlorosilane (n--C18H37SiHCl2).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04297499 |
| 출처 데이터셋 | uspto-grants-1981_10 |
| ORD ID | ord-752d3d99fdca4c918514c3964109bad8 |
| 출처 메모 | uspto-grants-1981_10 |