Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanol → trans-3-[2-(7-Chloroquinolin-2-yl)ethenyl]benzyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | Chloroform | HCID 6212 | — |
| 반응물 | trans-3-[2-(7-Chloroquinolin-2-yl)ethenyl]benzyl alcohol | HCID 10827738 | — |
| 용매 | Thionyl Chloride | HCID 24386 | — |
| 생성물 | trans-3-[2-(7-Chloroquinolin-2-yl)ethenyl]benzyl chloride | HCID 19369489 | — |
반응 단계
To a solution of 813 mg (2.75 mmol) of trans-3-[2-(7-chloroquinolin-2-yl)ethenyl]benzyl alcohol in 40 ml of CHCl3, 1.0 ml of SOCl2 was added, followed by stirring at room temperature for 24 hours. A small amount of MeOH was added to the reaction mixture and the solvent was distilled off under reduced pressure, whereby trans-3-[2-(7-chloroquinolin-2-yl)ethenyl]benzyl chloride was obtained as pale yellow powder.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06011033 |
| 출처 데이터셋 | uspto-grants-2000_01 |
| ORD ID | ord-4cb3d504de18416ea1c0eb408c2f02c8 |
| 출처 메모 | uspto-grants-2000_01 |