Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1) → HCID 54560967, 화합물
반응식
[C:1]1([CH:7]=[CH:8][CH2:9][CH:10]2[NH:16][C:15](=[O:17])[CH2:14][CH2:13][CH2:12][CH2:11]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.F[B-](F)(F)F.[CH3:23][O+](C)C>C(Cl)Cl>[CH3:23][O:17][C:15]1[CH2:14][CH2:13][CH2:12][CH2:11][CH:10]([CH2:9][CH:8]=[CH:7][C:1]2[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=2)[N:16]=1참가 물질
4
실험 절차
The title material of Example 32 (0.50 g, 2.2 mmol) in CH2Cl2 (15 mL) and in the presence of 3A molecular sieves (1.0 g) was reacted with trimethyloxonium tetrafluoroborate (0.39 g, 2.6 mmol) by the method of Example 3 to produce 0.53 g (99%) of the title material.
출처 및 근거
- ORD 기록
- ord-8f5e4843415d481098c2b8e8c9926d1f
- 출처 데이터셋
- uspto-grants-2000_01
- 특허 번호
- US06011028
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