Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → HCID 178479039, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | 6-Benzylpyridin-2-amine | HCID 93902 | — |
| 촉매 | Platinum oxide (PtO) | HCID 82844 | — |
| 생성물 | HCID 178479039 | HCID 178479039 | — |
반응 단계
The 2-amino-6-benzylpyridine was reduced as in Example 94, except platinum oxide was used as the catalyst. The product was obtained as an oil which was dissolved in 1 N HCl and lyophilized to give a white solid. The solid was recrystallized from EtOAc to give the desired title compound as white crystals. The analysis of the product was found to be consistent with the proposed structure.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06011028 |
| 출처 데이터셋 | uspto-grants-2000_01 |
| ORD ID | ord-ab961bebbe72482badb3276f57ec740a |
| 출처 메모 | uspto-grants-2000_01 |