Cyclobutanecarbonyl chloride → HCID 19367175, 화합물

반응식

[CH2:1]([CH:10]1[CH2:15][CH2:14][CH2:13][CH2:12][NH:11]1)/[CH:2]=[CH:3]/[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1.[CH:16]1([C:20](Cl)=[O:21])[CH2:19][CH2:18][CH2:17]1>>[CH2:1]([CH:10]1[CH2:15][CH2:14][CH2:13][CH2:12][N:11]1[C:20]([CH:16]1[CH2:19][CH2:18][CH2:17]1)=[O:21])/[CH:2]=[CH:3]/[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1

참가 물질

반응물 2

HCID 78705Cyclobutanecarbonyl chloride

HCID 10878208HCID 10878208, 화합물

생성물 1

HCID 19367175HCID 19367175, 화합물

실험 절차

Stage a) The method is the same as that of Example 1.1, Stage a), the initial reactants being (E)-2-(cinnamyl)piperidine and cyclobutanecarboxylic acid chloride, which furnish (E)-2-cinnamyl-1-(cyclobutanecarbonyl)piperidine (formula II; Ar=C6H5, m=1, n=2, R=cyclobutyl). Yield: 99%.

출처 및 근거

ORD 기록: ord-e5b1d089b9a543bdba2766df66d1d6e7
출처 데이터셋: uspto-grants-2000_01
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06013656

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