참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | ((Phenylthioxomethyl)thio)acetic acid | HCID 70336 | — |
| 반응물 | tert-Butylhydrazine monohydrochloride | HCID 81889 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | N'-t-butyl-N-(thiobenzoyl)hydrazine | HCID 19367775 | — |
반응 단계
S-(thiobenzoyl)thioglycolic acid (3.0 g) was dissolved in 20 ml pyridine, treated with t-butyl hydrazine hydrochloride (excess, ca. 4 g) and then was heated at ca. 120° C. for 14 hours. Water (120 ml) was added and the mixture was extracted with ether. The organic extracts were dried over anhydrous magnesium sulfate, filtered and evaporated to give crude N'-t-butyl-N-(thiobenzoyl)hydrazine as a viscous yellow oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06013836 |
|---|
| 출처 데이터셋 | uspto-grants-2000_01 |
|---|
| ORD ID | ord-94d56aaa95654b0b938589fcabec5f99 |
|---|
| 출처 메모 | uspto-grants-2000_01 |
|---|
