Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-(3-(Benzyloxy)phenyl)ethanamine → m-Tyramine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-(3-(Benzyloxy)phenyl)ethanamine | HCID 207415 | — |
| 반응물 | HCID 178418361 | HCID 178418361 | — |
| 촉매 | HCID 178418390 | HCID 178418390 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | m-Tyramine | HCID 11492 | 95.5% |
반응 단계
10% Palladium-carbon catalyst (water content 50%, 86 mg) was added to a solution of 2-(3-benzyloxyphenyl)ethylamine (434 mg, 1.91 mmol, 1.0 eq) in THF (10 ml), and the mixture was stirred at room temperature for 3 hours in a stream of hydrogen. The reaction ma ire was filtered through Celite, and the filtrate was concentrated under reduced pressure to give 2-(3-hydroxyphenyl)ethylamine (250 mg, 95.5%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06017919 |
| 출처 데이터셋 | uspto-grants-2000_01 |
| ORD ID | ord-a43b55be186346cb9f598980f7df62eb |
| 출처 메모 | uspto-grants-2000_01 |