N-[(E)-2,4-pentadienyl]-N-(2-propenyl)-acetamide → Non-2-ene

HRID 850713노트

반응식

HRID 850713 반응식
[CH2:1](N(CC=C)C(=O)C)/[CH:2]=[CH:3]/[CH:4]=[CH2:5]>C1(C)C(C)=CC=CC=1>[CH3:1][CH:2]=[CH:3][CH2:4][CH2:1][CH2:2][CH2:3][CH2:4][CH3:5]

참가 물질

3

반응물 1

HCID 12260271N-[(E)-2,4-pentadienyl]-N-(2-propenyl)-acetamide

생성물 1

HCID 33744Non-2-ene

시약·촉매·용매 1

HCID 7237O-Xylene용매

실험 절차

Dissolve 33.1 g (0.2 mol) of N-[(E)-2,4-pentadienyl]-N-(2-propenyl)-acetamide (title compound from Example A.3.) in 200 ml of xylene, pass a powerful stream of nitrogen through for 15 min, add 0.1 g of 4-hydroxyanisole, and then heat to reflux overnight. Concentrate, distil under high vacuum.

출처 및 근거

ORD 기록
ord-6b8caac8ed4444c5a1eb482c423281b5
출처 데이터셋
uspto-grants-2000_01
특허 번호
US06018054

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