Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic acid, bromo-, propyl ester → 10-bromo-2-n-propoxycarbonylmethyloxy-5-(3-pyridylmethyl)-4H-pyrido [3,2,1-jk]carbazole-4-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic acid, bromo-, propyl ester | HCID 141981 | — |
| 반응물 | 10-bromo-2-hydroxy-5-(3-pyridylmethyl)-4H-pyrido[3,2,1-jk]carbazole-4-one | HCID 15886910 | — |
| 생성물 | 10-bromo-2-n-propoxycarbonylmethyloxy-5-(3-pyridylmethyl)-4H-pyrido [3,2,1-jk]carbazole-4-one | HCID 15886914 | 55% |
반응 단계
The procedure of Example 3 was repeated by using 10-bromo-2-hydroxy-5-(3-pyridylmethyl)-4H-pyrido[3,2,1-jk]carbazole-4-one (250 mg) and n-propyl bromoacetate (0.1 ml) to obtain the title compound (170 mg, 55%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06018046 |
| 출처 데이터셋 | uspto-grants-2000_01 |
| ORD ID | ord-f19c4576aba94882bcb6692696660357 |
| 출처 메모 | uspto-grants-2000_01 |