Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sulfur trioxide → 2-Methyl-5-nitrobenzenesulfonic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sulfur trioxide | HCID 24682 | — |
| 반응물 | p-Nitrotoluene-2-sulphonic acid anhydride | HCID 53855915 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 2-Methyl-5-nitrobenzenesulfonic acid | HCID 8458 | — |
반응 단계
In this procedure, the reaction mixture is obtained as a black, tarry suspension towards the end of the addition of sulphur trioxide and, after hydrolysis of the p-nitrotoluene-2-sulphonic acid anhydride with water, an aqueous solution of p-nitrotoluene-2-sulphonic acid is formed from the suspension, and this is treated with active charcoal, before or after separating off water-insoluble by-products, in order to separate off dissolved, coloured compounds and dissolved, unreacted p-nitrotoluene.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04382039 |
| 출처 데이터셋 | uspto-grants-1983_05 |
| ORD ID | ord-917da601c499486f9e330177f0ceb84f |
| 출처 메모 | uspto-grants-1983_05 |