Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,3,4-Thiadiazol-2-amine → 2-(N-benzyloxycarbonyl-DL-isoleucylamino)-1,3,4-thiadiazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,3,4-Thiadiazol-2-amine | HCID 19909 | — |
| 반응물 | N-benzyloxycarbonyl-L-isoleucine | HCID 102945 | — |
| 생성물 | 2-(N-benzyloxycarbonyl-DL-isoleucylamino)-1,3,4-thiadiazole | HCID 13145510 | 56.6% |
반응 단계
26.5 g of N-benzyloxycarbonyl-DL-isoleucine and 10 g of 2-amino-1,3,4-thiadiazole were reacted in the same manner as in Example 3(i) to obtain 19.5 g (yield: 56%) of 2-(N-benzyloxycarbonyl-DL-isoleucylamino)-1,3,4-thiadiazole as white crystals having a melting point of 149° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04382142 |
| 출처 데이터셋 | uspto-grants-1983_05 |
| ORD ID | ord-867032a5d88647ba8c89db7026dadd3d |
| 출처 메모 | uspto-grants-1983_05 |