HCID 12428590, 화합물 → HCID 178457551, 화합물

반응식

[CH:1]([N:4]=[C:5]=[N:6][C:7]1[CH:8]=[N:9][CH:10]=[CH:11][CH:12]=1)([CH3:3])[CH3:2].C([N:17]=[C:18]=[N:19]C1C=NC=CC=1)(C)(C)C>>[C:18]([N:19]=[C:5]([NH:6][C:7]1[CH:8]=[N:9][CH:10]=[CH:11][CH:12]=1)[NH:4][CH:1]([CH3:3])[CH3:2])#[N:17]

참가 물질

반응물 2

HCID 12428590HCID 12428590, 화합물

HCID 20501927HCID 20501927, 화합물

생성물 1

HCID 178457551HCID 178457551, 화합물

실험 절차

By following the procedure of Example 1, but substituting N-isopropyl-N'-3-pyridylcarbodiimide for the N-tert-butyl-N'-3-pyridylcarbodiimide, the N"-cyano-N-isopropyl-N'-3-pyridylguanidine was obtained with a melting point of 154.5°-155.0° C. Warning: Strongly exothermic reaction was observed in this case.

출처 및 근거

ORD 기록: ord-abd9855267324408a277959248f1d055
출처 데이터셋: uspto-grants-1983_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: USRE031244

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