Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanimidic acid, N-phenyl-, ethyl ester → HCID 178482101, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanimidic acid, N-phenyl-, ethyl ester | HCID 111236 | — |
| 반응물 | HCID 178507418 | HCID 178507418 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | HCID 178482101 | HCID 178482101 | 56.9% |
반응 단계
Five grams of 4-(4-aminophenyl)-1-H-imidazole were added to a solution of 4.6 gm of ethyl N-phenyl-formimidate [Org. Synth., 35, 65 (1965)] in 25 ml of acetone. After stirring for four hours at room temperature, the solid that separated was filtered and dried under vacuum. The product was treated with acetone and acidified with glacial acetic acid. N-Phenyl-N'-[4-(imidazol-4-yl]-formamidine crystallized as acetate salt which was filtered to give 4.6 gm of the desired product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04386099 |
| 출처 데이터셋 | uspto-grants-1983_05 |
| ORD ID | ord-5cb2b46fd81545e6a611527823935340 |
| 출처 메모 | uspto-grants-1983_05 |