Methylamine → HCID 178484896, 화합물

HRID 851751노트

반응식

HRID 851751 반응식
[C:1]([NH:3][CH:4]=[N:5][C:6]1[CH:11]=[CH:10][C:9]([C:12]2[N:13]=[CH:14][NH:15][CH:16]=2)=[CH:8][CH:7]=1)#N.CN>O>[CH3:1][NH:3][CH:4]=[N:5][C:6]1[CH:11]=[CH:10][C:9]([C:12]2[N:13]=[CH:14][NH:15][CH:16]=2)=[CH:8][CH:7]=1

참가 물질

4

반응물 2

HCID 6329MethylamineHCID 178512241HCID 178512241, 화합물

생성물 1

HCID 178484896HCID 178484896, 화합물수율 70.9%

시약·촉매·용매 1

HCID 962Water용매

실험 절차

Twenty grams of N-cyano-N'-[4-(imidazol-4-yl)-phenyl]-formamidine was added in one portion to 35% methylamine in water (70 ml). A few minutes after the addition, the solid N-methyl-N'-[4-(imidazol-4-yl)-phenyl]-formamidine separated out of the solution. This solid was collected by filtration, washed with water, and dried to yield 13.45 gm of the desired product, which was recrystallized from acetone.

후처리

  1. additionA few minutes after the addition
  2. customthe solid N-methyl-N'-[4-(imidazol-4-yl)-phenyl]-formamidine separated out of the solution
  3. filtrationThis solid was collected by filtration
  4. washwashed with water
  5. customdried

출처 및 근거

ORD 기록
ord-c10122252efb46e1b065829d38281324
출처 데이터셋
uspto-grants-1983_05
특허 번호
US04386099

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