Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzene, 1-fluoro-2-methyl-4-nitro- → 3-({[tert-Butyl(diphenyl)silyl]oxy}methyl)-1-(2-methyl-4-nitrophenyl)pyridin-2(1H)-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzene, 1-fluoro-2-methyl-4-nitro- | HCID 68001 | — |
| 반응물 | 3-({[tert-Butyl(diphenyl)silyl]oxy}methyl)pyridin-2(1H)-one | HCID 59410156 | — |
| 생성물 | 3-({[tert-Butyl(diphenyl)silyl]oxy}methyl)-1-(2-methyl-4-nitrophenyl)pyridin-2(1H)-one | HCID 59410212 | — |
반응 단계
Analogously to Example 4A, 1.50 g (4.13 mmol) of the compound from Example 3A are reacted with 704 mg (4.54 mmol) of 2-fluoro-5-nitrotoluene. This gives 570 mg (28% of theory) of the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08846934B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-0bcd3dacdb0645a89ab81d6c03ce4396 |
| 출처 메모 | uspto-grants-2014_09 |