2-Pyridinecarboxaldehyde → HCID 9899550, 화합물

반응식

Cl[C:2]1[CH:3]=[C:4]([N:8]2[N:12]=[N:11][C:10]([C:13]3[CH:18]=[CH:17][CH:16]=[CH:15][N:14]=3)=[N:9]2)[CH:5]=[CH:6][CH:7]=1.[F:19]C1C=CC(NC2C=CC=CC=2)=CC=1.N1C=CC=CC=1C=O>>[F:19][C:7]1[CH:6]=[CH:5][C:4]([N:8]2[N:12]=[N:11][C:10]([C:13]3[CH:18]=[CH:17][CH:16]=[CH:15][N:14]=3)=[N:9]2)=[CH:3][CH:2]=1

참가 물질

반응물 3

HCID 142732-Pyridinecarboxaldehyde

HCID 27744684-Fluorodiphenylamine

HCID 99213692-[2-(3-chlorophenyl)-2H-tetrazol-5-yl]pyridine

생성물 1

HCID 9899550HCID 9899550, 화합물

실험 절차

Following the procedure described in EXAMPLE 1 for the synthesis of 2-[2-(3-chlorophenyl)-2H-tetrazol-5-yl]pyridine, 4-fluorophenylaniline (33.3 mg, 0.3 mmol) and 2-pyridinecarboxaldehyde (32.1 mg, 0.3 mmol) were employed to obtain 2-[2-(4-fluorophenyl)-2H-tetrazol-5-yl]pyridine as an orange solid.

출처 및 근거

ORD 기록: ord-0e590f413ec4421c89f90b824a372f5f
출처 데이터셋: uspto-grants-2007_08
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07253190B2

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