1-Chloro-4-iodobenzene → 2-{4-[5-(4-Chloro-phenyl)-pent-4-ynyloxy]-2-methyl-phenoxy}-2-methyl-propionic acid ethyl ester

HRID 852377노트

반응식

HRID 852377 반응식
[CH2:1]([O:3][C:4](=[O:22])[C:5]([CH3:21])([O:7][C:8]1[CH:13]=[CH:12][C:11]([O:14][CH2:15][CH2:16][CH2:17][C:18]#[CH:19])=[CH:10][C:9]=1[CH3:20])[CH3:6])[CH3:2].[Cl:23][C:24]1[CH:29]=[CH:28][C:27](I)=[CH:26][CH:25]=1>>[CH2:1]([O:3][C:4](=[O:22])[C:5]([O:7][C:8]1[CH:13]=[CH:12][C:11]([O:14][CH2:15][CH2:16][CH2:17][C:18]#[C:19][C:27]2[CH:28]=[CH:29][C:24]([Cl:23])=[CH:25][CH:26]=2)=[CH:10][C:9]=1[CH3:20])([CH3:21])[CH3:6])[CH3:2]

참가 물질

3

반응물 2

HCID 125101-Chloro-4-iodobenzeneHCID 866025402-Methyl-2-(2-methyl-4-pent-4-ynyloxy-phenoxy)-propionic acid ethyl ester

생성물 1

HCID 694589832-{4-[5-(4-Chloro-phenyl)-pent-4-ynyloxy]-2-methyl-phenoxy}-2-methyl-propionic acid ethyl ester

실험 절차

In analogy to the procedure described in example 13B], 2-methyl-2-(2-methyl-4-pent-4-ynyloxy-phenoxy)-propionic acid ethyl ester (example 13A]) and 1-chloro-4-iodo-benzene gave the title compound as a yellow viscous oil.

출처 및 근거

ORD 기록
ord-e9d572438ecf413cb46b52a59ce3ef99
출처 데이터셋
uspto-grants-2007_08
특허 번호
US07253192B2

반응 노트

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