2-Fluoro-3,5-dinitrobenzoic acid → Methyl 2-fluoro-3,5-dinitrobenzoate

반응식

[CH3:1][O:2][C:3](=[O:18])[C:4]1[CH:9]=[C:8]([N+:10]([O-:12])=[O:11])[C:7](OC)=[C:6]([N+:15]([O-:17])=[O:16])[CH:5]=1.[F:19]C1C([N+]([O-])=O)=CC([N+]([O-])=O)=CC=1C(O)=O>>[F:19][C:5]1[C:6]([N+:15]([O-:17])=[O:16])=[CH:7][C:8]([N+:10]([O-:12])=[O:11])=[CH:9][C:4]=1[C:3]([O:2][CH3:1])=[O:18]

참가 물질

반응물 2

HCID 6154042-Fluoro-3,5-dinitrobenzoic acid

HCID 14091421Methyl 4-methoxy-3,5-dinitrobenzoate

생성물 1

HCID 11064618Methyl 2-fluoro-3,5-dinitrobenzoate

실험 절차

Methyl 2-fluoro-3,5-dinitrobenzoate (D137) was prepared in an analogous manner to Description 25 (D25) from 2-fluoro-3,5-dinitrobenzoic acid (D136).

출처 및 근거

ORD 기록: ord-1691c1cfe47d402989300d9e1621110f
출처 데이터셋: uspto-grants-2007_08
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07253198B2

반응 노트

불러오는 중…