HCID 22936659, 화합물 → HCID 22936943, 화합물

HRID 853490노트

반응식

HRID 853490 반응식
[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:10](=[CH:11][C:12]=1[C:13]#[N:14])[N:9]=[CH:8][CH:7]=[C:6]2[O:15][C:16]1[CH:21]=[CH:20][C:19]([N+:22]([O-])=O)=[CH:18][CH:17]=1>[Fe]>[NH2:22][C:19]1[CH:18]=[CH:17][C:16]([O:15][C:6]2[C:5]3[C:10](=[CH:11][C:12]([C:13]#[N:14])=[C:3]([O:2][CH3:1])[CH:4]=3)[N:9]=[CH:8][CH:7]=2)=[CH:21][CH:20]=1

참가 물질

3

반응물 1

HCID 22936659HCID 22936659, 화합물

생성물 1

HCID 22936943HCID 22936943, 화합물수율 68.5%

시약·촉매·용매 1

HCID 23925Iron촉매

실험 절차

6-Methoxy-4-(4-nitrophenoxy)quinoline-7-carbonitrile (290 mg) was subjected to iron reduction by the same method as in Production Example 10 to obtain the title compound (180 mg).

출처 및 근거

ORD 기록
ord-aef6253888314229aba3fbb9dadde9e3
출처 데이터셋
uspto-grants-2007_08
특허 번호
US07253286B2

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