Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Quinoxaline-2-carbaldehyde → 2-Ethenylquinoxaline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Quinoxaline-2-carbaldehyde | HCID 594088 | — |
| 반응물 | 5-Ethenylpyrimidine | HCID 639849 | — |
| 생성물 | 2-Ethenylquinoxaline | HCID 21803421 | — |
반응 단계
Prepared in a similar manner to that described for Intermediate 2, replacing 2-vinylpyrazine with 2-vinylquinoxaline.* The product was purified by SPE using cyclohexane:ethylacetate (2:1 v/v) as eluent to provide the title compound as an oil. *{2-Vinylquinoxaline was synthesized from quinoxaline-2-carboxaldehyde using the procedure described in Intermediate 10 for 5-vinylpyrimidine}.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07259163B2 |
| 출처 데이터셋 | uspto-grants-2007_08 |
| ORD ID | ord-671bd50379a942d7b35f5a21fc1172a5 |
| 출처 메모 | uspto-grants-2007_08 |