반응식
CO[C:3]1[CH:4]=[CH:5][C:6]([O:11][CH2:12][O:13][CH3:14])=[C:7]([CH:10]=1)C=O.[OH:15][C:16]1C=CC(C=O)=CC=1>>[CH3:14][O:13][CH2:12][O:11][C:6]1[CH:7]=[CH:10][C:3]([CH:16]=[O:15])=[CH:4][CH:5]=1참가 물질
3
실험 절차
4-methoxymethoxybenzaldehyde (F3) was prepared in a similar manner for the preparation of 5-methoxy-2-methoxymethoxybenzaldehyde (F1) by using 4-hydroxybenzaldehyde (4.48 g, 40 mmol) instead of 2-hydroxy-5-methoxybenzaldehyde in 96% (6.40 g): 1H-NMR (500 MHz, CDCl3) δ3.53 (s, 1H), 5.24 (s, 2H), 7.17 (d, 1H, J=9.0 Hz), 7.35 (d, 1H, J=9.0 Hz), 10.52 (s, 1H).
출처 및 근거
- ORD 기록
- ord-bcf509a112dd4cd1abe99db8a4241f8e
- 출처 데이터셋
- uspto-grants-2007_08
- 특허 번호
- US07262301B1
연결된 노트
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