Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acrolein → N-(4-Chlorobenzylidene)-4-methylthioaniline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acrolein | HCID 7847 | — |
| 반응물 | alpha-(4-Chlorophenyl)-alpha-(4-methylthioanilino)acetonitrile | HCID 21862778 | — |
| 생성물 | N-(4-Chlorobenzylidene)-4-methylthioaniline | HCID 21862850 | — |
반응 단계
Following a procedure similar to that described in Example 21(iii), but using α-(4-chlorophenyl)-α-(4-methylthioanilino)acetonitrile [prepared as described in step (ii) above] and acrolein as starting materials, the title compound was obtained as an orange-colored powder (yield 32%), melting at 203-205° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | USRE039420E1 |
| 출처 데이터셋 | uspto-grants-2006_12 |
| ORD ID | ord-e8566af10da04d4cb67722f52d006b8e |
| 출처 메모 | uspto-grants-2006_12 |