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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 856822생성일: 2026년 10월 25일

4-(Methylthio)aniline → N-(4-difluoromethoxybenzylidene)-4-methylthioaniline

https://huagongshe.com/reaction/856822

반응식

참여 물질

역할이름HCID투입량
반응물4-(Methylthio)anilineHCID 66038—
반응물p-(Difluoromethoxy)benzaldehydeHCID 2736986—
생성물N-(4-difluoromethoxybenzylidene)-4-methylthioanilineHCID 2186282891%

반응 단계

Following a procedure similar to that described in Example 1(i), but using 4-difluoromethoxybenzaldehyde and 4-methylthioaniline as starting materials, N-(4-difluoromethoxybenzylidene)-4-methylthioaniline was obtained in a yield of 91%. This aniline compound and trimethylsilyl cyanide were then reacted together in a similar manner to that described in Example 1(ii), to give the title compound as a slightly yellow powder (yield 80%).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호USRE039420E1
출처 데이터셋uspto-grants-2006_12
ORD IDord-ab7bb03df30745508dffe4180a92fe44
출처 메모uspto-grants-2006_12