Sulfanilamide → 4-[(4-Ethoxybenzylidene)amino]benzenesulfonamide

반응식

[CH2:1]([O:3][C:4]1[CH:11]=[CH:10][C:7]([CH:8]=O)=[CH:6][CH:5]=1)[CH3:2].[S:12]([C:16]1[CH:22]=[CH:21][C:19]([NH2:20])=[CH:18][CH:17]=1)(=[O:15])(=[O:14])[NH2:13]>>[CH2:1]([O:3][C:4]1[CH:11]=[CH:10][C:7]([CH:8]=[N:20][C:19]2[CH:21]=[CH:22][C:16]([S:12](=[O:15])(=[O:14])[NH2:13])=[CH:17][CH:18]=2)=[CH:6][CH:5]=1)[CH3:2]

참가 물질

반응물 2

HCID 5333Sulfanilamide

HCID 248344-Ethoxybenzaldehyde

생성물 1

HCID 6908344-[(4-Ethoxybenzylidene)amino]benzenesulfonamide

실험 절차

Following a procedure similar to that described in Example 1(i), but using 4-ethoxybenzaldehyde and 4-sulfamoylaniline as starting materials, the title compound was obtained as a pale yellow powder (yield 76%).

출처 및 근거

ORD 기록: ord-f8f15591aa3440a688deab832d901bd4
출처 데이터셋: uspto-grants-2006_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: USRE039420E1

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