Barium nitrate → HCID 86587836, 화합물

HRID 856868

반응식

HRID 856868 반응식
[N+]([O-])([O-])=O.[Ba+2:5].[N+]([O-])([O-])=O.[CH2:10]([C:12]1[C:22]([C:23]([CH3:26])([CH3:25])[CH3:24])=[C:21]([OH:27])[C:20]([C:28]([CH3:31])([CH3:30])[CH3:29])=[CH:19][C:13]=1[CH2:14][P:15](=[O:18])([O-:17])[O-:16])[CH3:11].[Na+].[Na+]>>[CH2:10]([C:12]1[C:22]([C:23]([CH3:25])([CH3:24])[CH3:26])=[C:21]([OH:27])[C:20]([C:28]([CH3:29])([CH3:31])[CH3:30])=[CH:19][C:13]=1[CH2:14][P:15](=[O:16])([O-:18])[O-:17])[CH3:11].[CH2:10]([C:12]1[C:22]([C:23]([CH3:25])([CH3:24])[CH3:26])=[C:21]([OH:27])[C:20]([C:28]([CH3:29])([CH3:31])[CH3:30])=[CH:19][C:13]=1[CH2:14][P:15](=[O:16])([O-:18])[O-:17])[CH3:11].[Ba+2:5].[Ba+2:5]

참가 물질

3

반응물 2

HCID 24798Barium nitrateHCID 86587835Sodium (o-ethyl 3,5-di-tert-butyl-4-hydroxybenzylphosphonate)

생성물 1

HCID 86587836HCID 86587836, 화합물

실험 절차

5 ml aqueous solution of 392 mg (1.5 mmol) barium nitrate was added dropwise to 7.5 ml aqueous solution of 1 g (2.85 mmol) sodium (o-ethyl 3,5-di-tert-butyl-4-hydroxybenzylphosphonate) (phosphorus compound C described above) at room temperature under stirring. After the mixture was stirred for 1 hour, the precipitates were separated by filtration, washed with water and dried to give barium bis(o-ethyl 3,5-di-tert-butyl-4-hydroxybenzylphosphonate), 508 mg (45%).

후처리

  1. stirringAfter the mixture was stirred for 1 hour
  2. customthe precipitates were separated by filtration
  3. washwashed with water
  4. customdried

출처 및 근거

ORD 기록
ord-09e335155be044908b5cd50c70a075a6
출처 데이터셋
uspto-grants-2006_12
특허 번호
US07144614B2

연결된 노트

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