Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanol → N-[4-methoxy-4-(benzothiazol-2-yl)cyclohexa-2,5-dienylidene]4-methylbenzenesulphonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | N-[(4-benzothiazol-2-yl)phenyl]-4-methylbenzenesulfonamide | HCID 4380499 | — |
| 생성물 | N-[4-methoxy-4-(benzothiazol-2-yl)cyclohexa-2,5-dienylidene]4-methylbenzenesulphonamide | HCID 482713 | 73% |
반응 단계
To the the sulfonamide (0.1 g) dissolved in methanol (2 mL) was added BTIB (1.1 eq.) in one portion as a solid. The resulting suspension was stirred at room temperature for 5 hours. The precipitate formed was collected on a filter, washed with ice cold methanol (2 mL) and dried under vacuum to give the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07144893B2 |
| 출처 데이터셋 | uspto-grants-2006_12 |
| ORD ID | ord-b951bb7129ed40e7a6235adac8bb8d48 |
| 출처 메모 | uspto-grants-2006_12 |